
Sample recess
Theory assumes that the sample is placed coincident with the inside of the sphere wall,
however the sample is placed against the outside of the sphere wall. The porthole edges
have a finite thickness, and some part of the beam reflected at wide angles may be
intercepted by the sphere wall.
Figure 6: Some of the wide-angle reflection is intercepted by the sphere wall
The edges of the reflectance port are feathered to reduce this error.
Reference beam attenuation
Reference beam attenuation is most useful when the accessory or sample in the sample
beam attenuates the light beam considerably. In such situations, attenuation of the
reference beam will increase noise and considerably increase the dynamic range of the
instrument, as the detector is not then ’seeing’ two dramatically different signals. Clips are
provided at the reference beam window for this purpose. Metallic mesh screens are
recommended if reference beam attenuation is required (part number: 0110677500).
Stray light
If the irradiating beam overfills the reflectance port, a proportion of sphere wall
reflectance is mixed with that of the sample. This gives a high reading if this is not
consistent between the baseline and the sample measurement.
Gloss trap error
Gloss trap error is produced when the gloss trap is unable to completely absorb the
specular component. In the measurement of diffuse-only reflectance, a ’gloss trap’ is often
used to absorb the specular component. Gloss traps are typically glossy black pyramidal
light traps, matt black-coated cavities, or razor blade Fresnel light traps. However, the
reflectance of many samples has broadened the specular peaks which cannot be excluded
by standard sized light traps.
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